Journal Information
Vol. 8. Issue 3.
Pages 2481-2485 (May - June 2019)
Share
Share
Download PDF
More article options
Visits
852
Vol. 8. Issue 3.
Pages 2481-2485 (May - June 2019)
Original Article
DOI: 10.1016/j.jmrt.2019.02.002
Open Access
Influence of permanent magnetic fields on creep and microhardness of iron-containing aluminum alloy
Visits
852
Arkadiy A. Skvortsov
Corresponding author
skvortsovaa2009@yandex.ru

Corresponding author.
, Danila E. Pshonkin, Mikhail N. Luk’yanov, Margarita R. Rybakova
Department of Strength of Materials, Moscow Polytechnic University, Moscow, Russian Federation
This item has received
852
Visits

Under a Creative Commons license
Article information
Abstract
Full Text
Bibliography
Download PDF
Statistics
Figures (4)
Show moreShow less
Tables (1)
Table 1. The constants of aluminum alloy creep (r2 is the pair correlation coefficient).
Abstract

The necessity and urgency of studying plastic strain of metals is determined by both scientific significances of the problem and requirements of practice. So the objective of this work is investigation of aluminum alloy creep under action of static magnetic fields. This subject matter is of practical importance for engineering since the parts of engineering constructions are subject to various loads which may lead to their damage or even creep rupture. Based on the experiments performed by us, it is found that creeping increases under stable magnetic field; the main features appear at the first creep stage. Investigation of these processes will help to predict time dependence of creep strain and its rate as well as durability and plasticity at destruction.

Keywords:
Magnetoplastic effect
Aluminum alloys
Strain
Sample exposure
Mechanical tests
Full Text
1Introduction

It is known that influence of static magnetic field (MF) can change strain characteristics of a number of ionic, ionic-covalent, covalent, molecular and metal solids [1,2]. When discussing such issues, the so-called magnetoplastic effect (MPE) is often mentioned. MPE is a set of phenomena caused by dislocation motion in diamagnetic crystals under the action of external MF with induction of ∼1T and higher in the absence of deforming loads. MPE manifests itself as changes of mechanical characteristics of solids (plasticity, strength, plastic flow, etc.). They may either appear in the presence of MF or be long-term or even irreversible [1,2]. The effect of MF on plasticity of ferromagnetic materials is not considered in the present paper.

An analysis of MPE in diamagnetic crystals makes it possible to classify them in the following way [2]:

  • 1.

    Plasticity is changed only if the crystals are strained in MF. Presence of MF before or after strain does not change the mechanical properties of crystals [3,4]. As a rule, such materials demonstrate low sensitivity to temperature and high sensitivity to the type of impurity in the crystal.

  • 2.

    To make magnetic-stimulated effects appear, concurrent action of MF and an external exciting factor (e.g., electric current [5–7], ultrasound [8], etc.) is required.

  • 3.

    Plasticity of crystals can be changed by MF action before their strain (i.e., the residual changes initiated by MF remain) [9,10].

The effects related to the residual changes initiated by static MF are of considerable practical interest. At present the effect of preexposure to MF on metal plasticity is known [11]. A change of retardation of dislocations by magnetic-sensitive stoppers as a cause of metal softening after their preexposure to MF was considered in [1,2,9,11]. However, the performed experimental studies did not cover a wide range of the mentioned effects concerning aluminum and its alloys. There are no experimental results on the effect of static MF on creep of aluminum and its alloys Al-Mg-Si.

Therefore, the objective of the present work is experimental investigation of the effect of preexposure to MF of aluminum alloys on the processes of their creep.

2Materials and methods

For the experiments, we used standard flat aluminum samples with a width of 3.0mm in working section and a length of ℓo=80mm, which were cut from an aluminum strip 2mm thick. The material of the tape was an alloy of aluminum with magnesium and silicon Cal97.9%; CMg0.9%; CSi0.6%, CFe0.4%, other (Cu, Ti, Zn)0.2%). Other samples were cut from aluminum grade A99 with a content of CAl99.99%. Iron in aluminum was in the form of inclusions, the microstructure of the material and the deformation scheme are shown in Fig. 1. The strain of the elemental composition of the inclusion was carried out in the electron microscope column by Energy-dispersive X-ray spectroscopy (EDS).

Fig. 1.

SEM photomicrograph of the surface of an aluminum sample (a) containing Fe-inclusions 1 and a sample loading circuit (b). The arrow indicates the direction of the force F.

(0.14MB).

Samples were made of aluminum sheet by hydroabrasive cutting, which did not allow their strong heating. During the experiments, 45 samples were used, of which 25 were exposed to the field, and 20 – acted as witness specimens.

A magnetic field was created between poles of neodymium magnets. Induction of the magnetic field in the gap B=0.7T. When exposed, the lines of induction of the magnetic field were perpendicular to the plane of the sample. The exposure time ranged from 5min to 120min. Special studies have shown that the main changes occur during the first 10min of exposure in the MF. Further, the observed changes are practically independent of the exposure time. That is why in the work the time of the samples’ exposure to a magnetic field was 30min and always happened at room temperature [12].

Creep analysis was carried out on a test rig with a lever load system under conditions of normalized force during mechanical testing at room temperature. Preliminary measurements made it possible to determine the range of tensile loads (P=150…190N) when examining the creep of the samples described above.

3Results and discussion

It is known [13] that if static stretching force acts on a solid, then its crystal lattice will counteract to the applied force. Macroscopically this will be observed as strain (and subsequently destruction).

Metal creep can be described with a creep curve Δ(t) (Fig. 1). A strain Δo appears at loading and involves both plastic and elastic components [14]. A curve piece Δo…Δ1 (Fig. 1) at which creep rate is decreasing with time is the first creep stage. At the strain curve piece Δ1…Δ2 (Fig. 2) creep rate is insignificantly changed. A practically steady state is observed here. This curve piece is referred to as the second creep stage.

Fig. 2.

Aluminum alloy creep curves taken at a load P=170N at room temperature: 1, sample preexposure to static MF B=0.7T for 30min; 2, unexposed sample. Inset: a schematic of strain time dependence (creep curve) conventionally divided into three creep stages.

(0.12MB).

After strain Δ2, the third creep stage comes. The creep rate is gradually increasing until destruction occurs (at strain Δ3 and in the corresponding time t3). Therefore, the creep curves of aluminum alloy were registered only at the first and second creep stages.

Flat samples (length о=80mm, width of 3.0mm) cut from a band (thickness of 2mm) were used in experiments. The band material was an alloy of aluminum with magnesium and silicon: CAl97.9%; CMg0.9%; CSi0.6%, CFe0.4%, other (Cu, Ti, Zn)0.2%. MF was between the poles of neodymium magnets. MF induction B in the gap was of 0.7T. At exposure, the MF induction lines were perpendicular to the sample plane. The exposure time was varied from 5min to 120min. Special studies showed that the main changes occurred in the first 10min of exposure. Further observed changes practically did not depend on the exposure time. That is why the time of sample exposure to MF at room temperature always was 30min.

It was mentioned that in the present work creep processes were considered only at the first and second creep stages. The following relation is applicable to creep at perfect stretching known as “β-creep”. Under such conditions, the time dependence of relative strain ɛ=Δℓ/ℓ0 is [14]:

Here ɛо is relative strain immediately after start of loading; the constants β and m=1/3 are independent of loading time t[14]; k is creep rate at the second creep stage; Δ, Δо and o are absolute strain, that immediately after start of loading and initial sample length, respectively.

It is more conveniently to deal with absolute strain since just it is registered experimentally. So let us transform Eq. (1) into the following form:

Then we determine the constants in Eq. (2) (both before action of static MF and after it) using the experimental results on samples creep at different stretching loads (Р=150N…190N).

The typical experimental results obtained at stretching loads of 170N and 180N are presented in Figs. 1 and 2 (those obtained at the rest of loads do not differ principally from the above ones.) The results of creep curves approximation according to Eq. (2) are given in Table 1.

Table 1.

The constants of aluminum alloy creep (r2 is the pair correlation coefficient).

Parameter  Stretching load
  150N160N170N180N
B, T  0.7  0.7  0.7  0.7 
Δо, μm  428  469  490  529  554  748  818  1205 
β, 10−5, s−1/3  0.59  1.75  1.5  1.8  2.28  5.1  2.13  12.1 
K, 10−7, 1/s  1.25  1.25  1.38  2.01  0.25  2.30  0.60  1.00 
r2  0.975  0.978  0.896  0.897  0.956  0.986  0.987  0.999 

One can see that sample preexposure to static MF (induction B=0.7T) for 30min at room temperature promotes increasing of aluminum alloy strain practically in the whole range of applied stretching loads: immediately after start of loading ΔоВΔо=40μm at P=150N and ΔоВΔо=401μm at Р=180N. One should also note an appreciable effect of MF on the constant β: after “magnetic” exposure it is practically doubled at P=180N. At the same time, action of MF at the second creep stage practically does not change the creep rate constant k. This makes it possible to conclude that the results of samples preexposure to static MF manifest themselves most efficiently at the first creep stage.

The additional experimental arguments for the effect of static MF on the creep processes are presented in Fig. 3. It is not difficult to see that the difference in strains of the check test samples and the samples aged in MF increases with an external load. This is in agreement with the data given in Table 1 as well as those presented by other authors [1,2,15].

Fig. 3.

Aluminum alloy creep curves taken at a load P=180N at room temperature: 1, sample preexposure to static MF B=0.7T for 30min; 2, unexposed sample. Inset: a schematic of magnetic-stimulated strain ΔB on the applied stretching load P.

(0.11MB).

When discussing the assumed mechanisms of MF effect on plastic properties of magnesium-containing alloy, it is necessary to take into account one more factor related to presence of iron (up to 0.4%) in the aluminum alloy. Iron interacts with aluminum forming intermetallic phases [16]. Without silicon, the refractive phases Al3Fe and Al5Fe2 are predominant. However, the situation changes if silicon is present: the brittle α-phases Al8Fe2Si and Al5FeSi become predominant. If (just as in our case) magnesium is present (CMg0.9%), then π-phases Al8Fe3Mg3Si6 may appear in the aluminum alloy. The iron-containing intermetallic phases may be formed as plates (α-phase) and have ferromagnetic properties.

The purpose of the next part of the work was an experimental study of the effect of preliminary exposure of a constant magnetic field on the microhardness of an aluminum alloy studied earlier.

The microhardness was measured by pressing the Berkovich pyramid, while the load on the pyramid was 1N. As before, some of the samples were placed in a permanent magnetic field (B=0.7T, at room temperature) before mechanical tests. The measurement was carried out on 20 samples. The results of the studies showed that when measuring the microhardness on these samples, better reproducibility of the results was achieved at times of exposure to an indentor load of 5min or more. Therefore, the comparison of the results was carried out in the time range of 6–9min. The results obtained (Fig. 4) showed a significant difference in the values of the microhardness of samples that had been preliminarily exposed in MP (HV=310±30MPa) and the witness specimen (HV=420±30MPa).

Fig. 4.

Dependence of the microhardness of HV samples of an aluminum alloy on the time of loading on an indenter (P=1H) at room temperature: 1, preliminary exposure of samples in a constant magnetic field B=0.7T for 30min at room temperature; 2, specimen-witnesses without exposure in MP.

(0.11MB).
4Conclusion

Thus, the study of the influence of permanent magnetic fields on the creep of aluminum alloys was carried out. It was found experimentally that preliminary exposure of samples with a Fe content (∼0.4at. %) In a constant magnetic field (with induction B=0.7T for 30min at room temperature) leads to an increase in the absolute strain of the aluminum alloy to 35% and microhardness values. The experimentally weakened aluminum-based alloys after exposure in the MP can serve as an additional method for controlling the structurally sensitive properties of these materials.

Conflicts of interest

The authors declare no conflicts of interest.

Acknowledgment

This work was performed according to the project of the Ministry of Education and Science of Russian Federation (order No. 9. 8392.2017).

References
[1]
V.I. Alshits, E.V. Darinskaya, O.L. Kazakova, E.A. Petrzhik.
Magnetoplastic effect: basic properties and physical mechanisms.
Crystallogr Rep, 5 (2003), pp. 768-795
[2]
R.B. Morgunov.
Spin micromechanics in the physics of plasticity.
Phys Usp, 2 (2004), pp. 125-147
[3]
V.I. Alshits, E.V. Darinskaya, O.L. Kazakova, Mikhina EYu, E.A. Petrzhik.
Magnetoplastic effect in non-magnetic crystals and internal friction.
J Alloys Compd, 211–212 (1994), pp. 548-553
[4]
B.I. Smirnov, N.N. Peschanskaya, V.I. Nikolaev.
Magnetoplastic effect in NaNO2 ferroelectric crystals.
Phys Solid State, 12 (2001), pp. 2250-2252
[5]
A.A. Skvortsov, A.M. Orlov, V.A. Frolov, L.I. Gonchar, O.V. Litvinenko.
Influence of magnetic field on acoustic emission in dislocation-containing silicon under current loading.
Phys Solid State, 4 (2001), pp. 640-643
[6]
V.A. Makara, L.P. Steblenko, NYa. Gorid’ko.
On the influence of a constant magnetic field on the electroplastic effect in silicon crystals.
Phys Solid State, 3 (2001), pp. 480-483
[7]
A.R. Velikhanov.
Strain of Si under conditions of the combined influence of an electric current and a magnetic field.
Bull Russ Acad Sci Phys, 2 (2014), pp. 108-110
[8]
N.A. Tyapunina, V.L. Krasnikov, E.P. Belozerova, V.N. Vinogradov.
Effect of magnetic field on dislocation-induced unelasticity and plasticity of LiF crystals with various impurities.
Phys Solid State, 1 (2003), pp. 98-103
[9]
A.A. Skvortsov, A.V. Karizin, L.V. Volkova, M.V. Koryachko.
Effect of a constant magnetic field on dislocation anharmonicity in silicon.
Phys Solid State, 5 (2015), pp. 914-918
[10]
G.-R. Li, H.-M. Wang, P.-S. Li, Gao L-Zh, C.-X. Peng, R. Zheng.
Mechanism of dislocation kinetics under magnetoplastic effect.
Acta Phys Sin, 14 (2015), pp. 148102
[11]
Y. Li, Z. Luo, F. Yan, D. Rongquan, Y. Qi.
Effect of external magnetic field on resistance spot welds of aluminum alloy.
Mater Des, 56 (2014), pp. 1025-1033
[12]
L. Zhan, W. Li, Q. Ma, L. Liu.
The influence of different external fields on aging kinetics of 2219 aluminum alloy.
Metals, 6 (2016), pp. 201
[13]
G.F. Batalha, E.F. Prados, F.C. Ribeiro, B.T. Scarpin, D.J. Inforzato, P.R. Costa Jr., et al.
Creep age forming modeling and characterization.
Compr Mater Process, 2 (2014), pp. 149-159
[14]
F. Garofalo.
Fundamentals of creep and creep-rupture in metals.
MacMillan, (1968),
[15]
A.K. Soika, I.O. Sologub, V.G. Shepelevich, P.A. Sivtsova.
Magnetoplastic effect in metals in strong pulsed magnetic fields.
Phys Solid State, 10 (2015), pp. 1997-1999
[16]
G. Gottstein.
Physical foundations of material science.
Springer-Verlag, (2004),
Journal of Materials Research and Technology

Subscribe to our newsletter

Article options
Tools
Cookies policy
To improve our services and products, we use cookies (own or third parties authorized) to show advertising related to client preferences through the analyses of navigation customer behavior. Continuing navigation will be considered as acceptance of this use. You can change the settings or obtain more information by clicking here.